Cross-section polishing (CP) system utilizes broad argon ion beam (~1 mm) to mill away any materials that are not masked by the shield. It could produce a flat, smear-free cross sections readily be analyzed by SEM and electron backscattered diffraction (EBSD). The system is also equipped with cryogenic stage for preparation of temperature/beam sensitive samples. The cryo-stage is extremely useful for structural analysis of battery separators - cross-sectioning through ion milling at cryogenic temperature allows visualization of pore distribution without closing of pores due to local overheating.
CarlBerk’s central analytical lab is equipped with two different CP systems, a Gatan Ion II 697 model and a Leica EM TIC 3X system, both of which were installed with a build-in cryo-stage cooled by liquid nitrogen. Below are some representative cross-section samples prepared by CP systems.